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Open Source Apothecary At Home

Open Source Apothecary At Home / Preparations

Drying, and keeping a preparation good

Most of the strength of a home preparation is lost in the first month of bad storage, not in the making.

method

Two processes decide whether a dried herb is worth anything in six months: how it was dried, and how it is stored. Both are governed by the same chemistry — volatiles evaporate, phenolics oxidise, and water enables microbial growth and hydrolysis.

Drying. The target is below about 10% moisture for leaf and 12% for root, at which point the material snaps rather than bends. Two rules:

  • Heat drives off the volatile fraction. The compounds responsible for the smell of
  • Shade, not sun. Sunlight degrades chlorophyll and many phenolics, and the colour loss

Bundles or screens. Hanging small bundles in a dark, dry, ventilated room works well for stemmed herbs. Screens or trays work better for petals, leaf picked off the stem, and anything that would mould in a bundle. Either way, air must move — still air traps moisture in the middle of a bundle, and the middle of a bundle is where mould starts. Turn material daily in the first few days.

Harvest timing changes the chemistry, not just the yield. Secondary metabolite content peaks at a particular stage for each plant and part — commonly just before flowering for leaf, at full flower for flower, and in late autumn for root. Harvesting a leaf at the wrong stage gives a bigger pile of weaker material. Two practical markers: leaf before the plant flowers, flowers at their peak and in dry weather, and root after the tops have died back.

Storage. Four enemies, each with a specific counter:

| Enemy | Effect | Counter | |---|---|---| | Light | Degrades phenolics, bleaches | Amber or opaque glass, or a dark cupboard | | Oxygen | Oxidises oils and aromatics | Fill the jar high; minimise headspace | | Heat | Accelerates every degradation | Cool, stable temperature | | Moisture | Mould, hydrolysis, loss of potency | Absolutely dry herb in a sealed jar |

A sealed jar of genuinely dry herb in a dark cupboard keeps a useful phenolic content for 12-18 months; whole leaf keeps longer than powder because less surface is exposed. Powdered herb loses potency much faster than whole — one of the better arguments for storing leaf and grinding it as you use it. Roots and barks keep 2-3 years; flowers and volatile leaf 6-12 months.

The label is part of the method. Plant, part, date of harvest or purchase, and how it was dried. Without those, the second year's jar is an anonymous brown powder and the honest position is to throw it out.

Tests worth doing. Crush a leaf and smell it — if it is odourless it is spent. Look for a colour change toward brown or grey. Feel for any softness, which means moisture. Any mould, any musty smell, any clumping means discard: mycotoxins are not removed by washing or heating.

What the studies found

Comparative Study2018Food research international (Ottawa, Ont.)

Microencapsulation of betanin in monodisperse W/O/W emulsions.

Betanin increases the overall stability of the W/O/W emulsion, reduce the oil droplet size and improve size distribution when compared to the negative control without pigment and to emulsions containing betanin from other sources.
PubMed 29803475 ↗
Review2024Plant physiology and biochemistry : PPB

Harvest time optimization for medicinal and aromatic plant secondary metabolites.

Overall, our review provides valuable information for devising effective strategies to produce high-quality MAPs products.
PubMed 38781639 ↗
Review2022Mycorrhiza

Arbuscular mycorrhizal fungi and production of secondary metabolites in medicinal plants.

Medicinal plants are an important source of therapeutic compounds used in the treatment of many diseases since ancient times.
PubMed 35556179 ↗
Review2022Biomolecules

Recent Advances in Analytical Methods for the Detection of Olive Oil Oxidation Status during Storage along with Chemometrics, Authenticity and Fraud Studies.

Furthermore, the last part reflects on fraud in olive oil, and the most popular analytical techniques in the authenticity field are stated to highlight the importance of the authenticity of olive oil.
PubMed 36139019 ↗
Review2021Antioxidants (Basel, Switzerland)

Beneficial Role of Antioxidant Secondary Metabolites from Medicinal Plants in Maintaining Oral Health.

This review article contributes a basic outline of essential oils and their healing actions.
PubMed 34209152 ↗

Preparation

Air drying (best for volatile and delicate material)

  • Harvest on a dry morning after the dew has lifted, not after rain
  • Remove dead or damaged material; do not wash unless it is dirty, and if you wash it, dry
  • Bundle stems in small bunches (2-4 cm across) tied loosely, or lay leaf and petals on
  • Hang or place in a dark, dry, well-ventilated room at ambient temperature
  • Turn or rotate daily for the first 3-5 days
  • Ready when the material is brittle: leaf crumbles, stems snap, roots are hard
  • Expect 3:1 to 8:1 fresh-to-dry weight loss depending on the plant's water content

Dehydrator drying

  • 35-40 C for leaf, flower and anything aromatic
  • 45-55 C for root, bark and woody material, which has no volatiles to protect
  • Never use an oven above 60 C for aromatic material if you want it to still work

Roots specifically

  • Wash, then cut into 0.5-1 cm slices or split lengthwise; whole roots dry too slowly and
  • Dry at 45-55 C until a slice snaps cleanly and shows no soft core
  • This takes 1-3 days, not hours

Storage

1. Confirm dryness before jarring: material must snap, never bend. 2. Use glass with a gasket or a tight-fitting lid. Plastic bags are permeable to oxygen and to odour and are a storage method of last resort. 3. Label: plant, part, date, drying method. 4. Store in the dark at a stable cool temperature. A kitchen cupboard above a stove is the worst place in the house. 5. Check at 1 month and 3 months. If there is condensation inside the jar, the herb was not dry enough — take it out, dry it again, and re-jar. 6. Working lives: flowers and volatile leaf 6-12 months; other leaf 12-18 months; root and bark 2-3 years; powdered herb, half of those figures.

Infused oils and salves

  • Dark glass, filled high, cool and dark
  • 12 months for an oil; 6-12 months for a salve
  • Discard at any smell of old nuts or crayons, or a tacky texture — that is rancidity, and

Tinctures

  • Amber dropper bottles; 3-5 years
  • Re-check the ethanol percentage by nose — a tincture that has lost its alcohol smell has

Cautions and interactions

Related

Sources

  1. Microencapsulation of betanin in monodisperse W/O/W emulsions. Food research international (Ottawa, Ont.) 2018; doi:10.1016/j.foodres.2018.04.053 PubMed 29803475
  2. Harvest time optimization for medicinal and aromatic plant secondary metabolites. Plant physiology and biochemistry : PPB 2024; doi:10.1016/j.plaphy.2024.108735 PubMed 38781639
  3. Arbuscular mycorrhizal fungi and production of secondary metabolites in medicinal plants. Mycorrhiza 2022; doi:10.1007/s11104-015-2388-6 PubMed 35556179
  4. Recent Advances in Analytical Methods for the Detection of Olive Oil Oxidation Status during Storage along with Chemometrics, Authenticity and Fraud Studies. Biomolecules 2022; doi:10.1039/C5AY01765C PubMed 36139019
  5. Beneficial Role of Antioxidant Secondary Metabolites from Medicinal Plants in Maintaining Oral Health. Antioxidants (Basel, Switzerland) 2021; doi:10.1016/j.cmi.2021.05.028 PubMed 34209152